Rules and regulations pertaining to use of NMR
instruments are as follows. If you have any questions about them,
or would like to receive training in the use of the NMR equipment,
please contact
Dr. Greg Wylie
in Room 376.
Access to NMR Facility
1. Every person who wants to use a spectrometer must be explicitly
authorized to do so by the NMR Facility staff. This "explicit
authorization" will include a check-out test in which the
person demonstrates to NMR staff that he/she can use the spectrometer
in question, without assistance from another person, and without
endangering either themselves or the spectrometer. Unauthorized
use of the spectrometers will result in suspension of, or refusal
to grant, user privileges.
2. All NMR tubes should be 8in in length and 5mm OD. Only Wilmad
528-PP-8 (precision tube 8 in), WG-1241-8 (economy tube 8 in)
or better NMR tubes, or their equivalent, are approved for use
in this NMR Facility. Tubes must be kept externally CLEAN! The
"thrift" NMR is not allowed in any of the NMR spectrometers.
In addition, any NMR tube which does not fit properly into the
spinner turbine is not allowed. We strongly recommend the use
of Wilmad 535PP tubes for Varian Inova500, Wilmad 528PP tubes
for Varian MercuryPlus 400. The use of a substandard and/or dirty
NMR tube can damage the NMR spectrometer's probe. Probe damage
and instrument downtime resulting from the use of a substandard
NMR tube will be charged to the research group responsible for
the damage. Use of substandard and/or dirty NMR tubes in the spectrometers
will result in suspension of user privileges.
3. Metal objects are NOT allowed in any of NMR labs. Bringing
metal objectives such as keys, tools close to magnets could seriously
damage the magnets.
4. Food and drink are not allowed
in any of NMR labs.
5. No one is allowed to wear lab gloves
when operating NMR instrument.
Reservation of NMR Time for the 500 MHz.
1. NMR users reserving time need to go to http://faces.ccrc.uga.edu/
using group name UGACHEM_NMR. Username and password can be obtained
by sending a request to Dr.
Wylie. You must have a UGA email address in order to have
an access to the NMR schedule system.
2. The minimum block of time an operator may reserve is 20 minutes.
This is also the minimum amount of time for which the operator's
research group will be charged.
3. NMR users must start work no later than fifteen minutes after
the beginning of their reserved time, otherwise their entire reservation
will revert to open time. NMR users may not run over more than
ten minutes into another user's reservation. NMR users who repeatedly
inconvenience others by running late and/or not using their reserved
time will be denied use of the NMR facility.
Reservation of NMR Time for the 400 MHz.
1. The 400 spectrometer is available as a 'walk-up' instrument
with no reservation needed. This 'walk-up' usage will be restricted
to 35 minutes per submission between the hours of 8am and 9pm.
After 9pm there is no time restriction for Walk-up usage will
be unavailable during periods of instrument maintenance and training.
NMR Training
1. Training of new NMR users will be provided by NMR
Manager. Please visit NMR homepage at www.uga.edu/nmr and click
on Training for more information.
2. A new NMR user must read and understand the "Rules and
Regulations" (this document) to be authorized to use NMR
equipment at the NMR Facility.
3. It is highly recomended that users take the NMR course that
is offered in the Fall semestar.